EnglishA supercritical fluid extraction-supercritical fluid chromatography system coupled off-line with FT-IR spectrometry is described. The effects of pressure, temperature and time on the efficiency of the extraction of PCBs in certified and spiked soil samples were studied. A typical recovery of 75 % with a relative standard deviation of 7 % was obtained. The identity of chromatographic peaks was found by comparing their infrared spectra with reference spectra obtained from standard Aroclor solutions.
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http://hdl.handle.net/11568/17519| Autori interni: | FUOCO, ROGER |
| Autori: | FUOCO R; GRIFFITHS PR |
| Titolo: | ANALYSIS OF POLYCHLOROBIPHENYLS (PCBS) IN CONTAMINATED SOIL SAMPLES BY SUPERCRITICAL FLUID EXTRACTION SUPERCRITICAL FLUID CHROMATOGRAPHY COUPLED WITH FT-IR SPECTROMETRY |
| Anno del prodotto: | 1992 |
| Appare nelle tipologie: | 1.1 Articolo in rivista |
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