The protonated lactam salts [ ]2[MoOCl5], 2, and [ ]2[MoOCl4{ }]Cl, 3, were isolated from, respectively, the 1:2 and 1:3 molar ratio reactions of molybdenum pentachloride with -valerolactam in dichloromethane, and were characterized by X-ray diffraction, analytical and spectroscopic techniques.
Lactam/MoCl5 Interaction in CH2Cl2: synthesis and X-ray Characterization of Protonated -Valerolactam Salts
MARCHETTI, FABIO;PAMPALONI, GUIDO;
2013-01-01
Abstract
The protonated lactam salts [ ]2[MoOCl5], 2, and [ ]2[MoOCl4{ }]Cl, 3, were isolated from, respectively, the 1:2 and 1:3 molar ratio reactions of molybdenum pentachloride with -valerolactam in dichloromethane, and were characterized by X-ray diffraction, analytical and spectroscopic techniques.File in questo prodotto:
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