A new synthetic approach to aryl and alkyl alpha,beta-unsaturated sulfoxides is reported. The reaction has been optimized with respect to solvent, temperature, and ratio of reagents. The described procedure allows the synthesis of the title compounds in good yields (71-82%) starting from readily available reagents, in a cost-effective procedure.
Reinheckel protocol revisited: Synthesis of (E)-alpha,beta-unsaturated sulfoxides
Signore, Giovanni;SAMARITANI, SIMONA;MALANGA, CORRADO;MENICAGLI, RITA
2006-01-01
Abstract
A new synthetic approach to aryl and alkyl alpha,beta-unsaturated sulfoxides is reported. The reaction has been optimized with respect to solvent, temperature, and ratio of reagents. The described procedure allows the synthesis of the title compounds in good yields (71-82%) starting from readily available reagents, in a cost-effective procedure.File in questo prodotto:
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