ThepresentworkreportsastraightforwardapproachforthemechanochemicaloxidativenitrosoDiels–Alder(DA)reactionforthe rapidsynthesisofoxadiazo[2.2.2]octenesandamechanochemical[3+3]hetero-Coperearrangementtoaccessthecorresponding dioxazineswithinreducedreactiontime(upto1.5minand1.5h,respectively),highyieldsandreproducibilitytowarddifferent functionalgroups.
Mechanochemical Synthesis and Functionalization of Oxadiazo[2.2.2]octenes Through Oxidative Nitroso Diels–Alder Reaction and Hetero‐Cope Rearrangement
Caterina Campinoti;Simona Marchetti;Mauro Pineschi;Fabio Bellina
;Antonio Del Vecchio
;Marco Lessi
2026-01-01
Abstract
ThepresentworkreportsastraightforwardapproachforthemechanochemicaloxidativenitrosoDiels–Alder(DA)reactionforthe rapidsynthesisofoxadiazo[2.2.2]octenesandamechanochemical[3+3]hetero-Coperearrangementtoaccessthecorresponding dioxazineswithinreducedreactiontime(upto1.5minand1.5h,respectively),highyieldsandreproducibilitytowarddifferent functionalgroups.File in questo prodotto:
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